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Ultra-precision ductile grinding of BK7 using super abrasive diamond wheel

ZHAO Qingliang, Brinksmeier Ekkard, Riemer Oltmann, Rickens Kai

《机械工程前沿（英文）》 2007年第2卷第3期页码 350-355 doi: 10.1007/s11465-007-0061-3

摘要： In this paper, a novel conditioning technique using copper bonded diamond grinding wheels of 91 yD grain size and electrolytic in-process dressing (ELID) is first developed to precisely and effectively condition a nickel-electroplated monolayer coarse-grained diamond grinding wheel of 151 μm grain size. Under optimised conditioning parameters, the super abrasive diamond wheel was well conditioned in terms of a minimized run-out error and flattened diamond grain surfaces of constant peripheral envelope. The conditioning force was monitored by a force transducer, while the modified wheel surface status was in-situ monitored by a coaxial optical distance measurement system. Finally, the grinding experiment on BK7 was conducted using the well-conditioned wheel with the corresponding surface morphology and subsurface damage measured by atomic force microscope (AFM) and scanning electric microscope (SEM), respectively. The experimental result shows that the newly developed conditioning technique is applicable and feasible to ductile grinding optical glass featuring nano scale surface roughness, indicating the potential of super abrasive diamond wheels in ductile machining brittle materials.

关键词： ELID peripheral electrolytic in-process nickel-electroplated monolayer measurement

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Numerical investigation on side heat transfer enhancement in 300 kA aluminum reduction cell

WANG Changhong, ZHU Dongsheng, LEI Junxi, ZHOU Jiemin

《能源前沿（英文）》 2008年第2卷第3期页码 256-260 doi: 10.1007/s11708-008-0051-0

摘要： Industrial test and numerical simulation were synchronously applied to analyze the side heat transfer process and enhance heat transfer in aluminum reduction cell. The 3D slice finite element model of aluminum reduction cell was developed, with which the sidewall temperature field of the cell was computed by using software ANSYS. The main influencing factors on heat dissipation were analyzed and some effective measures were proposed to enhance sidewall heat transfer. The results show that the shell temperature of the test cell and the common cell is respectively 312°C and 318°C and the ledge thickness is 16 cm and 15 cm when side coefficient of heat transfer between the shell and the surroundings is 70 W/(mK). With the increase of the side coefficient of heat transfer between the shell and the surroundings, the temperature of the shell decreases but the thickness of the side ledge increases when the electrolytic temperature, the ambient temperature, the coefficient of heat transfer between molten bath and ledge, the eutectic temperature and the thermo-resistance of the side lining are constant.

关键词： constant ambient temperature thickness electrolytic temperature transfer process

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21世纪伊始铝电解工业的新进展

邱竹贤

《中国工程科学》 2003年第5卷第4期页码 41-46

摘要：

21世纪伊始，法国500kA特大型预焙阳极电解槽，以及中国320 kA大型电解槽的出现，标志着铝电解工业的重要新进展。文章从理论上分析了大型电解槽的优越性，论述了减少电解槽的热损失系数，即减少按单位电量核算的热损失量，便是大型槽能够节省电能的理论基础；应用低温铝电解和惰性电极是铝电解工业今后的发展方向。

关键词：铝电解工业大型电解槽低温铝电解惰性阳极和惰性阴极

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非并网风电电解水制氢系统及应用研究

颜卓勇,孔祥威

《中国工程科学》 2015年第17卷第3期页码 30-29

摘要：

2013年中国风电新增装机容量为16.1 GW，累计装机容量为91.42 GW，两项指标均居世界第一，却有大量风机不能并网发电。当前，并网难已成为我国大规模风电发展中的突出问题。非并网风电是指风电系统的终端负荷不再是传统的单一电网，而是通过必要的技术创新与集成，直接应用于一系列能适应风电特性的高载能产业及其他特殊领域。在江苏大丰市建成日产120 Nm3非并网风电电解水制氢系统示范工程。该系统利用1台30 kW风机和1台10 kW风机共同给电解水制氢装置供电，采用非并网风电供电模式，风电联网不并网，消除了风电对电网的冲击，实现风电100 %高效、低成本利用。该系统的研究可以揭示风电与电解水制氢工艺之间的耦合规律。

关键词：非并网；风电；电解水制氢

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电解锰行业污染防治最佳可行技术评估及污染减排潜力

李旭华,方刚,党春阁,于秀玲

《中国工程科学》 2013年第15卷第3期页码 56-61

摘要：

电解锰行业废水排放量大，污染物浓度高，属于高污染行业，是我国实现污染物控制减排的主要威胁之一。通过对电解锰行业污染防治现状进行分析，构建了污染防治技术评估指标体系，利用层次分析法确定各评价指标的权重，利用综合评价值法对电解锰行业污染防治技术进行了评估。在此基础上，利用自底向上模型对评估出的最佳可行技术的污染减排潜力进行预测。结果表明，与基准年2010年相比，2015年电解锰行业废水排放总量可削减270多万吨，氨氮减排6.6×104 t，减排回收的锰和重铬酸钾可分别达到1.9×105 t和3.747×107 t，锰渣减排4×106 t；同时也表明清洁生产技术减排的能力高于末端治理技术减排，清洁生产技术具有较大的推广普及潜力。

关键词：电解锰污染防治最佳可行技术减排潜力

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Applications of the crystallization process in the pharmaceutical industry

Sohrab ROHANI

《化学科学与工程前沿（英文）》 2010年第4卷第1期页码 2-9 doi: 10.1007/s11705-009-0297-z

摘要： The applications of the crystallization technique in the pharmaceutical industry as a purification and separation process for the isolation and synthesis of pure active pharmaceutical ingredients (API), co-crystals, controlled release pulmonary drug delivery, and separation of chiral isomers are briefly discussed using a few case studies. The effect of process variables and solvent on the polymorphism and morphology of stavudine is discussed. The implementation of external control in the form of feedback and real-time optimal control using cooling and antisolvent crystallization of paracetamol in water-isopropyl alcohol is introduced. Two methods to prepare micron-sized drug particles, namely, micro-crystallization and polymer-coated API-loaded magnetic nanoparticles for pulmonary drug delivery, are discussed. The significance of co-crystals in drug administration is highlighted using the theophylline-nicotinamide co-crystal system. Resolution of chloromandelic acid derivatives, a racemic compound, is achieved using direct crystallization and diastereomeric salts crystallization. The crystal structures of diastereomeric salts of chloromandelic acid and phenylethylamine are determined. The structure comparison between the less soluble and more soluble salts shows that weak interactions such as CH/π interactions and van der Waals forces contribute to chiral recognition when the hydrogen bonding patterns are similar.

关键词： feedback morphology pulmonary paracetamol recognition

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Degradation of refractory organics in concentrated leachate by the Fenton process: Central compositedesign for process optimization

Senem Yazici Guvenc, Gamze Varank

《环境科学与工程前沿（英文）》 2021年第15卷第1期 doi: 10.1007/s11783-020-1294-1

摘要： Abstract • 90% total COD, 95.3% inert COD and 97.2% UV254 were removed. • High R2 values (over 95%) for all responses were obtained with CCD. • Operational cost was calculated to be 0.238 €/g CODremoved for total COD removal. • Fenton oxidation was highly-efficient method for inert COD removal. • BOD5/COD ratio of leachate concentrate raised from 0.04 to 0.4. The primary aim of this study is inert COD removal from leachate nanofiltration concentrate because of its high concentration of resistant organic pollutants. Within this framework, this study focuses on the treatability of leachate nanofiltration concentrate through Fenton oxidation and optimization of process parameters to reach the maximum pollutant removal by using response surface methodology (RSM). Initial pH, Fe2+ concentration, H2O2/Fe2+ molar ratio and oxidation time are selected as the independent variables, whereas total COD, color, inert COD and UV254 removal are selected as the responses. According to the ANOVA results, the R2 values of all responses are found to be over 95%. Under the optimum conditions determined by the model (pH: 3.99, Fe2+: 150 mmol/L, H2O2/Fe2+: 3.27 and oxidation time: 84.8 min), the maximum COD removal efficiency is determined as 91.4% by the model. The color, inert COD and UV254 removal efficiencies are determined to be 99.9%, 97.2% and 99.5%, respectively, by the model, whereas the total COD, color, inert COD and UV254 removal efficiencies are found respectively to be 90%, 96.5%, 95.3% and 97.2%, experimentally under the optimum operating conditions. The Fenton process improves the biodegradability of the leachate NF concentrate, increasing the BOD5/COD ratio from the value of 0.04 to the value of 0.4. The operational cost of the process is calculated to be 0.238 €/g CODremoved. The results indicate that the Fenton oxidation process is an efficient and economical technology in improvement of the biological degradability of leachate nanofiltration concentrate and in removal of resistant organic pollutants.

关键词： Concentrated leachate Fenton oxidation Central composite design Biodegradability Inert COD

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Review on mechanism and process of surface polishing using lasers

Arun KRISHNAN, Fengzhou FANG

《机械工程前沿（英文）》 2019年第14卷第3期页码 299-319 doi: 10.1007/s11465-019-0535-0

摘要： Laser polishing is a technology of smoothening the surface of various materials with highly intense laser beams. When these beams impact on the material surface to be polished, the surface starts to be melted due to the high temperature. The melted material is then relocated from the ‘peaks to valleys’ under the multidirectional action of surface tension. By varying the process parameters such as beam intensity, energy density, spot diameter, and feed rate, different rates of surface roughness can be achieved. High precision polishing of surfaces can be done using laser process. Currently, laser polishing has extended its applications from photonics to molds as well as bio-medical sectors. Conventional polishing techniques have many drawbacks such as less capability of polishing freeform surfaces, environmental pollution, long processing time, and health hazards for the operators. Laser polishing on the other hand eliminates all the mentioned drawbacks and comes as a promising technology that can be relied for smoothening of initial topography of the surfaces irrespective of the complexity of the surface. Majority of the researchers performed laser polishing on materials such as steel, titanium, and its alloys because of its low cost and reliability. This article gives a detailed overview of the laser polishing mechanism by explaining various process parameters briefly to get a better understanding about the entire polishing process. The advantages and applications are also explained clearly to have a good knowledge about the importance of laser polishing in the future.

关键词： laser polishing surface roughness process parameters mechanism

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Tool path strategy and cutting process monitoring in intelligent machining

Ming CHEN, Chengdong WANG, Qinglong AN, Weiwei MING

《机械工程前沿（英文）》 2018年第13卷第2期页码 232-242 doi: 10.1007/s11465-018-0469-y

摘要：

Intelligent machining is a current focus in advanced manufacturing technology, and is characterized by high accuracy and efficiency. A central technology of intelligent machining—the cutting process online monitoring and optimization—is urgently needed for mass production. In this research, the cutting process online monitoring and optimization in jet engine impeller machining, cranio-maxillofacial surgery, and hydraulic servo valve deburring are introduced as examples of intelligent machining. Results show that intelligent tool path optimization and cutting process online monitoring are efficient techniques for improving the efficiency, quality, and reliability of machining.

关键词： intelligent machining tool path strategy process optimization online monitoring

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Seasonal and treatment-process variations in invertebrates in drinking water treatment plants

Zhiling Wu, Xianchun Tang, Hongbin Chen

《环境科学与工程前沿（英文）》 2021年第15卷第4期 doi: 10.1007/s11783-020-1354-6

摘要： Abstract • Seasonal and treatment-process variations in invertebrates in a DWTP were analyzed. • The propagation and leakage of invertebrates in BAC filter were the most serious. • Invertebrates can survive and reproduce in chlorine disinfected clear water tanks. • Proportions of endogenous invertebrates increased along the treatment process. Problems associated with excessive propagation and leakage of invertebrates in drinking water have received increasing attention in recent years. We performed a monthly survey of invertebrate abundance and taxa in the effluent of each treatment stage in a drinking water treatment plant between May 2015 and April 2016 and analyzed seasonal and treatment-process variations in invertebrates. The results showed that invertebrate abundances in raw water, effluent of the biological activated carbon (BAC) filter, and finished water significantly correlated with water temperature, whereas no correlation was observed between water temperature and invertebrate abundance in the effluents of the sedimentation tank and sand filter. The dominant taxa in the effluent of each treatment stage were rotifers, nematodes, and crustaceans. The sedimentation tank could efficiently remove invertebrates with an annual average removal rate of 92%. The propagation and leakage of invertebrates occurred in the sand and BAC filters but more seriously in the latter. The average reproduction rate in the BAC filter was 268.8% with rotifers as the taxon that leaked the most. Invertebrate survival and reproduction were also observed in the chlorine-disinfected clean water reservoir with an average reproduction rate of 41.9%. Owing to differences in chlorine resistance, the reproduction ability of the dominant taxa was in the order nematodes>crustaceans>rotifers. The proportion of endogenous invertebrates gradually increased along the treatment process. The average proportion of endogenous invertebrates in the finished water was higher than 79.0%. Our findings suggested that waterworks should pay more attention to endogenous invertebrate growth.

关键词： Invertebrates Drinking water Seasonal variations Treatment process

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Special issue on “Green chemical process and intensification”

《化学科学与工程前沿（英文）》 2022年第16卷第11期页码 1533-1535 doi: 10.1007/s11705-022-2263-y

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Electrolytic cell engineering and device optimization for electrosynthesis of e-biofuels via co-valorisation

Faraz Montazersadgh, Hao Zhang, Anas Alkayal, Benjamin Buckley, Ben W. Kolosz, Bing Xu, Jin Xuan

《化学科学与工程前沿（英文）》 2021年第15卷第1期页码 208-219 doi: 10.1007/s11705-020-1945-6

摘要： Utilizing CO in an electro-chemical process and synthesizing value-added chemicals are amongst the few viable and scalable pathways in carbon capture and utilization technologies. CO electro-reduction is also counted as one of the main options entailing less fossil fuel consumption and as a future electrical energy storage strategy. The current study aims at developing a new electrochemical platform to produce low-carbon e-biofuel through multifunctional electrosynthesis and integrated co-valorisation of biomass feedstocks with captured CO . In this approach, CO is reduced at the cathode to produce drop-in fuels (e.g., methanol) while value-added chemicals (e.g., selective oxidation of alcohols, aldehydes, carboxylic acids and amines/amides) are produced at the anode. In this work, a numerical model of a continuous-flow design considering various anodic and cathodic reactions was built to determine the most techno-economically feasible configurations from the aspects of energy efficiency, environment impact and economical values. The reactor design was then optimized via parametric analysis.

关键词： electrosynthesis e-biofuels CO₂ utilization computational model

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Sulfate digestion process for high purity TiO

T. A. LASHEEN

《化学科学与工程前沿（英文）》 2009年第3卷第2期页码 155-160 doi: 10.1007/s11705-009-0005-z

摘要： A titania slag product of Rosetta ilmenite assaying 72% TiO is treated by the sulfate process option of the pigmentary TiO manufacture. The relevant factors of acid concentration, particle size, slag/acid ratio besides the reaction temperature, and time have been studied. After dissolving the cured mass in dilute acid and clarification, the obtained solution was subjected to hydrolysis of its titanium content. The final product was bleached under reducing conditions to redissolve the residual coloring impurities before being dewatered and calcinated. The obtained results indicated that a leaching efficiency of about 92% was realized due to the presence of some refractory components in the working slag material, namely, rutile and magnesium iron titanate. The obtained white pigment assay attained up to 99.85% TiO , while the analyzed impurities involve 77 ppm Mn and only 14 and 7 ppm of total iron and V, respectively.

关键词： titania slag sulfate process pigment

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Multiscale process systems engineering—analysis and design of chemical and energy systems from moleculardesign up to process optimization

《化学科学与工程前沿（英文）》 2022年第16卷第2期页码 137-140 doi: 10.1007/s11705-021-2135-x

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A stepwise process for carbon dioxide sequestration using magnesium silicates

Johan FAGERLUND, Experience NDUAGU, Ron ZEVENHOVEN, Inês ROMÃO,

《化学科学与工程前沿（英文）》 2010年第4卷第2期页码 133-141 doi: 10.1007/s11705-009-0259-5

摘要： This work involves the production of magnesium in the form of Mg(OH) from serpentinite rock (nickel mine tailing) material followed by conversion into MgCO using a pressurised fluidised bed (PFB) reactor operating at 400°C–600°C and pressures up to 2.85MPa. Our approach is rooted in the thermodynamic fact that the reaction between Mg(OH) and gaseous CO forming MgCO and water releases significant amounts of heat. The main problem is, however, the chemical kinetics; the reaction is slow and has to be accelerated in order to be used in an economically viable process for large-scale (~1Mt/a) CO sequestration. We have constructed a lab-scale PFB reactor test-setup for optimising the carbonation reaction. At high enough temperatures and conversion levels the reaction should provide the heat for the proceeding Mg(OH) production step, making the overall process energy neutral. So far we have been able to achieve a conversion degree of 26% at 500°C and 2.85MPa after 30min (particle size 125–212μm). In this paper the test facility and our latest results and progress on CO mineral carbonation are summarised. Also, the possible integration of the iron as a feedstock for iron and steel production will be briefly addressed. An interesting side-effect of this carbon dioxide capture and storage (CCS) route is that significant amounts of iron are obtained from the serpentinite rock material. This is released during the Mg(OH) production and can be of great interest to the iron- and steel producing sector, which at the same time is Finland’s largest CO producer.

关键词： carbonation reaction reactor producer large-scale process